Download e-book for kindle: Analytical Profiles of Drug Substances, Vol. 2 by FLOREY KLAUS

By FLOREY KLAUS

ISBN-10: 012260802X

ISBN-13: 9780122608025

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AMPICILLIN The optical rotation for ampicillin trihydrate, /-&26 + 2 4 5 . 0) has been reported62. 7O (C = 1, buffer pH 8 . 0 p . Optical rotation in 2 1 hydrochloric acid, after dissolution of 1% ampicillin and 60 minutes of standing at 25OC is = -85. 5°C64. 3. 1 Modes of Penicillin Degradation The main course of deterioration penicillins is hydrolysis. The course of the hydrolysis is shown in Figure 9. Dunham65 reviewed modes of penicillin degradation. 23 F i g u r e 9. O. Wilson, 0. Gisvol and R .

39. 40. 41. 42. 43. 44. M o r i n , R . B. , J a c k s o n , B . G . , M u e l l e r , R . A . , L a v a g n i n o , E . R . B. a n d Andrews. S . L . , J . A m . Chem. S O C . , 91, 1 4 0 1 ( 1 9 6 9 ) . J . , “ T h e I n f r a r e d S p e c t r a o f Complex M o l e c u l e s . ” M e t h u e n , Lo n d o n , 2nd e d . , 1 9 5 8 , p. 214. W a y l a n d , L. a n d W e i s s . P . J . J . A s s o c . Chem. 48 ( 5 ) . 965 ( 1 9 6 5 ) . , Page J . E . , and S t a n i f o r t h . S . W . , J . Chem.

7 0 , 57722m ( 1 9 6 9 ) . N o v a k , L . , K o e n i g , J. a n d R u d i n g e r , J . , C z e c h . 1 2 4 , 8 3 6 , O c t o b e r 1 5 , 1 9 6 7 : C . A . -96 9 96706h ( 1 9 6 8 ) . E k s t r o m , B. a n d S j o b e r g , B . , A c t a C h e m . Scand. 19, 1245 ( 1 9 6 5 ) . B i a n c h i , G. a n d Z a n n i n i , E . , S . A f r i c a n 70 7 7 9 5 5 t 6 8 0 0 , 2 9 4 , J u l y 9 , 1968: C . A . (1969). A l b u r n , H . E . , C l a r k , D . E . S. 3 , 5 2 0 , 8 7 6 , J u l y 2 1 , 1 9 7 0 : C .

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Analytical Profiles of Drug Substances, Vol. 2 by FLOREY KLAUS


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